Distillation Test Methods in Petroleum Products

This test method is one of the oldest petroleum test methods and is a way to quantitatively determine the boiling range of petroleum products with a minimum drying point of 2 degrees Celsius. These include jet fuel, gasoline, kerosene, gas oil, petroleum solvents, a variety of naphtha and the like (distillate fuels).

This method is not applicable for products containing significant residual material. In this method, the sample is subdivided into one of the four groups defined in this standard based on the volatility and vapor pressure, initial boiling point or expected endpoint, or both, and is distilled under the specific test conditions of that group.

At ambient pressure, it is approximately equivalent to a fractional distiller with a theoretical plate. At the end of distillation, the observed steam temperatures can be corrected to atmospheric pressure and the data obtained to conform to the requirements of the test method (such as distillation velocities) and the test should be repeated if any of the conditions are not met. . The test results are reported as percent evaporated or recovered percent relative to the respective temperature, in a table or in a graph on a distillation curve diagram.

Technical Specifications

SPECIFICATIONS

Discharge temperature Oil and oil products with a boiling point
of +18 to +400 ° C
Speed ​​of distillation Automatic maintenance of the distillation rate depending on the selected test program in the range 2 to 10 ml / min
Oil product groups dark oil products, oil, paraffin oil, paraffins according to GOST 2177 (ISO 3405) Method B;1, 2, 3, 4 according to GOST 2177 (ISO 3405) Method A;

1, 2, 3, 4 according to GOST R EN ISO 3405;

1, 2, 3, 4 according to ASTM D 86.

PRECISION CHARACTERISTICS
The volume of the distilled product, ml ± 0.3
Product vapor temperature from 0 to 300: ± 1.0, from 300 to 400: ± 1.5
Barometric pressure ± 1
Cooling bath temperature from 0 to 60: ± 0.5
Receiver temperature from 13 to 60: ± 0.5
Speed ​​of distillation, ml / min from 0 to 9: ± 0.5
OPERATING CHARACTERISTICS
Power Consumption not more than 1500 V · A
Dimensions 750 x 585 x 515 mm (height x width x depth)
Weight not more than 50 kg (without taking into account the coolant in the bath)
Ambient temperature +15 to +35 ° C
Relative humidity not more than 75%
Voltage from 187 to 242 V
Frequency from 49 to 51 Hz
Life time 6 years, no more than 15 000 hours
Warranty period of operation 1 year, not more than 2 500 hours
(does not apply to glassware)
Life time 6 years, no more than 15 000 hours
Warranty period 1 year, not more than 2 500 hours

video

Pre-invoice application form